Obtaining zeolite A from filtrate of zeolite LSX and its influence on the removal of heavy metals and organic pollutants in spent lubricating oil

R. Kwakye; A. Aniagyei; B. Kwakye-Awuah; B. Y. Vibgedor; B. O. Asimeng

doi:10.1590/0366-69132021673833108

Obtaining zeolite A from filtrate of zeolite LSX and its influence on the removal of heavy metals and organic pollutants in spent lubricating oil

R. Kwakye, A. Aniagyei, B. Kwakye-Awuah, B. Y. Vibgedor, B. O. Asimeng

Department of Biomedical Engineering

Research output: Contribution to journal › Article › peer-review

3 Citations (Scopus)

Abstract

Zeolites A was synthesized from alternate sources such as filtrate from synthesized zeolite LSX and aluminate solution extracted from bauxite which produced a very good yield. The synthesized zeolite type was characterized by X-ray diffractometry (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDX). The synthesized product showed a high degree of crystallinity from the XRD results. When applied to a spent lubricating oil, the efficiency in removing the heavy metals was: 23.4% Fe, 96.8% Zn, 19.0% Cu, and 12.0% Cr. The saturates in the regenerated oil were 80% carbon, 4% residue, and 16% aromatics as compared to that of a commercial virgin oil that contained 84% saturates, 3% carbon residue, and 13% aromatics. This indicated that the spent oil can be reused.

Original language	English
Pages (from-to)	284-288
Number of pages	5
Journal	Ceramica
Volume	67
Issue number	383
DOIs	https://doi.org/10.1590/0366-69132021673833108
Publication status	Published - Jul 2021

Keywords

Aromatics
Lubricating oil
Saturates
Synthesis
Zeolites

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10.1590/0366-69132021673833108

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@article{1550d71158054593866cc1fd672bf407,

title = "Obtaining zeolite A from filtrate of zeolite LSX and its influence on the removal of heavy metals and organic pollutants in spent lubricating oil",

abstract = "Zeolites A was synthesized from alternate sources such as filtrate from synthesized zeolite LSX and aluminate solution extracted from bauxite which produced a very good yield. The synthesized zeolite type was characterized by X-ray diffractometry (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDX). The synthesized product showed a high degree of crystallinity from the XRD results. When applied to a spent lubricating oil, the efficiency in removing the heavy metals was: 23.4\% Fe, 96.8\% Zn, 19.0\% Cu, and 12.0\% Cr. The saturates in the regenerated oil were 80\% carbon, 4\% residue, and 16\% aromatics as compared to that of a commercial virgin oil that contained 84\% saturates, 3\% carbon residue, and 13\% aromatics. This indicated that the spent oil can be reused.",

keywords = "Aromatics, Lubricating oil, Saturates, Synthesis, Zeolites",

author = "R. Kwakye and A. Aniagyei and B. Kwakye-Awuah and Vibgedor, \{B. Y.\} and Asimeng, \{B. O.\}",

year = "2021",

month = jul,

doi = "10.1590/0366-69132021673833108",

language = "English",

volume = "67",

pages = "284--288",

journal = "Ceramica",

issn = "0366-6913",

publisher = "Associacao Brasileira de Ceramica",

number = "383",

}

TY - JOUR

T1 - Obtaining zeolite A from filtrate of zeolite LSX and its influence on the removal of heavy metals and organic pollutants in spent lubricating oil

AU - Kwakye, R.

AU - Aniagyei, A.

AU - Kwakye-Awuah, B.

AU - Vibgedor, B. Y.

AU - Asimeng, B. O.

PY - 2021/7

Y1 - 2021/7

N2 - Zeolites A was synthesized from alternate sources such as filtrate from synthesized zeolite LSX and aluminate solution extracted from bauxite which produced a very good yield. The synthesized zeolite type was characterized by X-ray diffractometry (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDX). The synthesized product showed a high degree of crystallinity from the XRD results. When applied to a spent lubricating oil, the efficiency in removing the heavy metals was: 23.4% Fe, 96.8% Zn, 19.0% Cu, and 12.0% Cr. The saturates in the regenerated oil were 80% carbon, 4% residue, and 16% aromatics as compared to that of a commercial virgin oil that contained 84% saturates, 3% carbon residue, and 13% aromatics. This indicated that the spent oil can be reused.

AB - Zeolites A was synthesized from alternate sources such as filtrate from synthesized zeolite LSX and aluminate solution extracted from bauxite which produced a very good yield. The synthesized zeolite type was characterized by X-ray diffractometry (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDX). The synthesized product showed a high degree of crystallinity from the XRD results. When applied to a spent lubricating oil, the efficiency in removing the heavy metals was: 23.4% Fe, 96.8% Zn, 19.0% Cu, and 12.0% Cr. The saturates in the regenerated oil were 80% carbon, 4% residue, and 16% aromatics as compared to that of a commercial virgin oil that contained 84% saturates, 3% carbon residue, and 13% aromatics. This indicated that the spent oil can be reused.

KW - Aromatics

KW - Lubricating oil

KW - Saturates

KW - Synthesis

KW - Zeolites

UR - https://www.scopus.com/pages/publications/85116689366

U2 - 10.1590/0366-69132021673833108

DO - 10.1590/0366-69132021673833108

M3 - Article

AN - SCOPUS:85116689366

SN - 0366-6913

VL - 67

SP - 284

EP - 288

JO - Ceramica

JF - Ceramica

IS - 383

ER -

Obtaining zeolite A from filtrate of zeolite LSX and its influence on the removal of heavy metals and organic pollutants in spent lubricating oil

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Keywords

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